Production Equipment

Reactors:
800 liter QVF/DeDietrich glass-lined reactor. Heating/cooling unit Huber unistat 645w. Temperature interval: -40°C – 200°C
250 liter Buchi glass-lined reactor. Heating/cooling unit Huber unistat 166w. Temperature interval: -50°C – 200°C
50 liter Buchi glass-lined reactor. Heating/cooling unit Huber unistat 164w. Temperature interval: -50°C – 200°C
2×20 liter Diehm glass reactors. Heating/cooling unit Huber CC75. Temperature interval: -75°C – 100°C
20 liter Diehm glass reactor. Heating/cooling unit Huber Unistat 140W HT. Temperature interval: -40°C – 150°C
5 liter Diehm glass reactor. Heating/cooling unit Julabo FP50. Temperature interval: -35°C – 150°C

Pressure reactors:
100 liter Buchi pressure reactor. Heating/cooling unit Huber unistat. Temperature interval: -40°C – 200°C
20 liter Buchi pressure reactor. Heating/cooling unit Huber CC75. Temperature interval: -75°C – 100°C. Max pressure: 10 bar
3 liter Buchi pressure reactor. Heating/cooling unit Huber CC75. Temperature interval: -75°C – 100°C. Max pressure: 6 bar

Distillation equipment:
VTA short-path evaporator. Operating pressure: atmosphere to 0.001 mbar Working temperature: max 300 °C (evaporator). Throughput 0.1 to 2 L per hour

Preparative HPLC systems
Gram-scale system: Shimadzu LC-8A gradient pump with UV-Vis detector and fraction collector. Standard Column: KR100-10-C18, 20.8 × 250 mm
Kilogram-scale system: Varian SD-2 Varian UV with UV-Vis and ELSD detectors. Binary gradient up to 1.2 L/min. Standard Columns: Varian DAC/SAC columns; i.d. 50 and 150, length 50 to 400 mm.

Nutsche filters:
150 liter stainless steel nutsche filter with lid
2×30 liter stainless steel nutsche filter with lid
10 liter PTFE coated stainless steel nutsche filter with lid
30 liter Aurora filter (model A20-S) used for contained filtration and drying. Equipped with PSL charging point with butterfly valve. Heating/cooling unit Huber. Temperature interval: -75°C – 100°C